Martensitic Anisotropy Measurements

Ni2MnGa Martensitic Anisotropy Measurements

The martensitic anisotropy measurements were designed to determine the anisotropy constant for a single variant of Ni2MnGa martensite. The strategy of the tests was to compress the specimen into a single variant microstructure using the small fixture shown to the right, and generate M-H curves parallel and perpendicular to the compression axis as shown. The fixture was constructed from a non-magnetic CuBe spring alloy and sized to fit in the cooling fixture used with the VSM. Stress was applied to the specimen with the small set screw; the amount of extension set with the screw controlled the load applied to detwin the specimen on cooling below Ms, and also determined the amount of stress present on the single variant specimen after transformation. The applied stress in the single variant state was an important parameter in the tests, for it was required to prevent the nucleation of a second variant for applied fields perpendicular to the compression axis (far right figure), and also allowed for a determination of the ordinary magnetostriction constant from stress anisotropy effects.

This graph shows the M-H curve performed at -17°C with 1.9 MPa applied stress. The results show that the easy axis within a single variant is the c-axis as expected, and the anisotropy is uniaxial in nature. Uniaxial anisotropy constant Ku was calculated from the areas between these 2 curves and found to be Ku=2.4 x 106 ergs/cc. M-H curves taken at additional stress values allowed for a calculation of the magnetostriction constant for a single variant of martensite (next section)


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